A kind of complex Copper slag has been studied. The runofmine grade of copper was %. Through the research of the flotation separation test, the optimal grinding fineness () was about to 75%. The optimum kind and dosage of collector was 150 g/t Y89. The dosage of sodium silie which was the Slime dispersing agent was 1000g/t. The dosage of sodium carbonate was 800g/t.